
R&D World Online - April 2020
Ultra-Low Vibration Lab facilitates nanoengineering discoveries
            by Steve Varma, Operations Manager, Minus K Technology
            Posted By Heather Hall | April 15, 2020
          
      
The Ultra-Low Vibration Lab is a part of the new Center of  Excellence in Nano Mechanical Science and Engineering (NAMSE) – a recent  addition to the G.G. Brown Laboratories on the North Campus of the University  of Michigan in Ann Arbor.
Noel Perkins, former associate chair for Facilities and Planning  with the Department of Mechanical Engineering, describes this addition as a  “building-within-a-building”. The Nanoengineering Lab, located on the ground  floor, contains eight ultra-low-vibration chambers for nanoscale metrology,  mechanical, temperature and interference testing.
  
The  chambers are structurally isolated from the balance of the building.   Vibration isolation tables are mounted on pillars that are part of an  8-ft-thick seismic mass, which is isolated from the chamber floors. Even  researchers’ footsteps won’t disturb experiments. “With the emergence of  nanotechnology and nanoengineering of the last two decades, a relatively small  number of institutions and agencies have been able to construct facilities for  ultra-sensitive measurements, and I know of none that are focused on the  mission of a mechanical engineering department,” said Edgar Meyhofer, professor  of mechanical engineering and biomedical engineering at the university.
  
  
  Meyhofer, in conjunction with Pramod Reddy, a professor of  mechanical engineering, and materials science and engineering at the University  of Michigan, have been collaborating on nanoscale heat transfer, energy  transduction and biomechanics research. Other researchers are utilizing the  Nanostructures Lab to build artificial platelet cells for medical purposes and  artificial neurons for advanced computers. While at the University’s  Microdynamics Lab, the tiniest forces are studied, utilizing computational  models that describe the mechanics of DNA and protein assemblies, and the  behavior of viruses.
  
  Since the opening of ULVL in 2014, two  major scientific milestones have been achieved: 
  1)      Measuring heat fluxes at the  nanoscale, thereby validating fluctuational electrodynamics;
  2)      Establishing that light emitting  diodes (LEDs) can be used to cool electronic devices in supercomputers.
  Validating Fluctuational  Electrodynamics 
  When heat travels between two separated objects, it flows  differently at the smallest scales – distances on the order of the diameter of  DNA, or 1/50,000 of a human hair. For example, heat radiates 10,000 times  faster at the nanoscale. Researchers have been aware of this for decades,  but they have not understood the process. Now, at ULVL, researchers have  measured how heat radiates from one surface to another in a vacuum at distances  down to 2 nanometers.
  "We've shown for the first time, the dramatic enhancements of  radiative heat fluxes in the extreme near-field," said Reddy. "Our  experiments and calculations imply that heat flows several orders of magnitude  faster in these ultra-small gaps."
  Reddy and Meyhofer led the work.  A paper on the findings was  recently published in the international journal of science, Nature.
In the middle of the last century, the Russian radio physicist, Sergei Rytov,  proposed a new theory called “fluctuational electrodynamics” to describe heat  transfer at smaller than 10-micrometer distances. Since then, research hasn’t  always resulted in supporting evidence.
  
  “Experiments were undertaken in the 1990s and early 2000s that  tried to test these ideas further, and they found large discrepancies between  what theory would predict and what their experiments revealed,” explained  Meyhofer.  Because of the sophistication of the University of Michigan’s  new laboratory, the researchers say their findings close the case, and Rytov  was right.
  
  
  The ULVL chamber was custom designed for performing nanoscale  experiments, so precise, that they are sensitive to mere footsteps.  The vibration isolation system in the chamber consists of a  seismic mass and a sophisticated low-vibration table, which reduces vibrations  from outside, and inside, such as mechanical vibrations associated with heating and cooling systems, or elevators.
  
  The chamber limits acoustic noise, temperature and humidity  variations, as well as radio frequency and magnetic interference. “Our facility  represents the true state-of-the-art,” Meyhofer said.  “When creating  nanoscale gaps, such as those required for our nanoscale heat radiation  experiments, the slightest perturbation can ruin an experiment.”
  
  In the chamber, the researchers use custom-built “scanning thermal  microscopy probes” that allowed them to directly study how fast heat flows  between two surfaces of silica, silicon nitride and gold.  The researchers  chose these materials because they are commonly used in nanotechnology.
  
  For each material, they designated one sample (the planar  substrate) that would be heated to 305°F.  Using a probe, they coated the  tip with the same material, but kept it connected at the base to a thermal  reservoir that was maintained at a cooler 98°F. The sample and the probe were  slowly moved, together, in small steps, beginning at 50 nanometers until they  were touching.  The temperature of the tip was measured at regular  distances (gaps) between 2 nm and 50 nm. The cause of the rapid heat transfer,  the researchers discovered, was the result of an overlap of the two sides’  surfaces, and evanescent waves, both of which carry heat. A phenomenon present  in nanoscale gaps.
  
  “These waves reach only a small distance into the gap between  materials,” said Bai Song, a former graduate student in mechanical engineering  and one of the lead authors. “And their intensity at the extreme near-field is  enormous compared to the electromagnetic waves at larger distances. When these  waves from the two different devices overlap, that is when they allow  tremendous heat flux.”
  
Cooling Supercomputers with Heat-Absorbing LEDs 
  LEDs with electrodes can reverse-cool adjoining devices a mere few  nanometers away.  This approach could lead to new solid-state cooling technology for future  microprocessors, which will have so many transistors packed into small spaces  that current methods will be incapable of removing heat quickly enough.   "We have demonstrated a second method for using photons to cool devices,"  said Reddy, who co-led this work with Meyhofer. "The LED, with this  reverse bias trick, behaves as if it were at a lower  temperature.”
  
  Measuring this cooling, and proving that anything interesting has  occurred, is considerably complicated. To get enough infrared light to flow  from an object into the LED, the two would have to be extremely close together,  less than a single wavelength of infrared light. This is necessary to take  advantage of near field or evanescent coupling effects, which enable more  infrared photons to cross from the object to be cooled into the LED.
  
  Reddy and Meyhofer had an advantage, as they had already been  heating and cooling nanoscale devices, arranging them so that they were only a  few tens of nanometers apart.  At this close proximity, a photon, that  would not have escaped the object to be cooled, can pass into the LED, almost  as if the gap between them did not exist.
  
  These experiments became possible because the team had access to  the ULVL ultra-low vibration laboratory, where measurements of objects  separated by nanometers become feasible because vibrations are dramatically  reduced.
  
  The group proved the principle by building a minuscule  calorimeter, which is a device that measures changes in energy, and putting it  next to a tiny LED about the size of a grain of rice. They were constantly  emitting and receiving thermal photons from each other and elsewhere in their  environments.
  
  "Any object that is at room temperature is emitting light,”  Meyhofer said.  “For example, a night vision camera is basically capturing  the infrared light that is coming from a warm body.”
  
  Once the LED was reverse-biased, it began acting as a very-low  temperature object, absorbing photons from the calorimeter.  At the same  time, the gap prevents heat from traveling back into the calorimeter via  conduction, resulting in a cooling effect.
  
  The team demonstrated cooling of 6 watts per meter squared.  Theoretically, this effect could produce cooling equivalent to 1,000 watts per  meter squared, or about the power of sunshine on the Earth's surface.
  
  This research could turn out to be important for future  smartphones and other computers. With more computing power in smaller and  smaller devices, removing heat from the microprocessor is beginning to limit  how much power can be squeezed into a given space.  With improvements in  the efficiency and cooling rates of this new approach, the team envisions this  phenomenon as a way to quickly draw heat away from microprocessors in  devices.  It could even stand up to the abuses endured by smartphones, as  nanoscale spacers could provide the separation between microprocessor and LED.
  
  Engineering a Solution for  the Ultra-Low Vibration Lab
  After the construction phase of the Center of Excellence in NAMSE  was completed, a vibration survey was done on the Ultra-Low Vibration Lab  chambers. The measurements demonstrated that even when a single vehicle was  driving on a nearby street, the vibrations exceeded the NIST-A specifications  necessary for the ULVL.
  
  In order for the Ultra-Low Vibration Lab to be successful it was required to have a Vibration Criterion (VC) of NIST-A (1 µm, 1 – 20 Hz; 125 µm  between 20 – 100 Hz). The VC criteria were developed in the early 1980s by Eric  Ungar and Colin Gordon. They were originally developed for use in the  semiconductor industry but have found application in a wide variety of  technological applications. The NIST-A criterion was developed for metrology  but has gained popularity within the nanotechnology community.
  
  The recommendations to achieve the required specifications included controlling traffic on nearby streets in direct proximity of the new  building addition, as well as upgrading the planned pneumatic vibration  isolators on optical tables with Negative-Stiffness isolators, designed and  manufactured by Minus K Technology.
  The University of Michigan ordered seven customized tabletops and  31 custom Minus K Negative-Stiffness vibration isolators with pedestals  provided for the eight Ultra-Low Vibration Lab chambers.
Negative-Stiffness  isolators employ a unique and completely mechanical concept in low-frequency  vibration isolation. They do not require electricity or compressed air. There  are no motors, pumps, or chambers, and no maintenance because there is nothing  to wear out. They operate purely in a passive mechanical mode.
  
  
“In this vibration isolation system, vertical-motion isolation is  provided by a stiff spring that supports a weight load, combined with a  Negative-Stiffness mechanism,” explained Dr. David Platus, President of Minus K  Technology. “The net vertical stiffness is made very low without affecting the  static load-supporting capability of the spring. Beam-columns connected in  series with the vertical-motion isolator provide horizontal motion isolation. A  beam-column behaves as a spring combined with a negative-stiffness mechanism.”
  
  The isolator provides 0.5 Hz isolation performance vertical and  horizontal. Note that for an isolation system with a 0.5 Hz natural frequency,  isolation begins at about 0.7 Hz and improves with increase in the vibration  frequency. The natural frequency is more commonly used to describe the system  performance.
  
  Negative-stiffness isolators resonate at 0.5 Hz. At this frequency  there is almost no energy present. It would be very unusual to find a  significant vibration at 0.5 Hz. Vibrations with frequencies above 0.7 Hz  (where negative-stiffness isolators begin isolating) are rapidly attenuated  with increase in frequency.
  
  Transmissibility with negative-stiffness isolators is  substantially improved over air systems. Transmissibility is a measure of the  vibrations that are transmitted through the isolator relative to the input  vibrations.
  
  The Negative-Stiffness isolators, when adjusted to 0.5 Hz, achieve  93% isolation efficiency at 2 Hz; 99% at 5 Hz; and 99.7% at 10 Hz.  Negative-Stiffness isolators deliver very high performance, as measured by a  transmissibility curve.
  
  
  Record-Low VC-M Vibration  Level 
  The final vibration survey by internationally recognized vibration  and acoustics consultant Colin Gordon Associates (CGA), after installation of  the customized Minus K Negative-Stiffness isolators and tables, showed the  measured vibration levels in all ULVL chambers from VC-K to VC-M at frequencies  above 2.5 Hz. Vibration criterion (VC) curves are commonly used in the  evaluation of the ambient vibration of facilities. 
  "VC-M is the lowest we have ever measured, though we weren’t  able to measure below 2.5 Hz because our most sensitive sensor won’t go lower,  due to sensor noise floor," said Hal Amick, Vice President of Colin Gordon  Associates. The measurements by CGA revealed that the tables provide isolation  between 1.25 and 160 Hz, at least 10dB above 2 Hz, 20dB above 4 Hz and 80Hz.  This is remarkable, given the low noise environment in which these tables have  to perform.   
 
 
			 
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